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Methylsulfonyl, -trifluoromethylsulfonyl, -tolylsulfonyl, -benzylsulfonyl, -allylsulfonyl, -benzylsulfonyl, -benzyloxylsulfonyl, -vinylsulfonyl, -p-toluenesulfonyl, -acenaphthene-2-sulfonyl and -salicyl-2-sulfonyl carboxylates were prepared and utilized to evaluate the capacity of these reagents to activate iodonium (alkylsulfonyl) carboxylates for reaction with aryl halides. These sulfonyl carboxylates, under anhydrous conditions, were found to effectively oxidize iodonium alkylsulfonyl carboxylates in a 1:1 reaction mixture in acetonitrile, provided the sulfonyl reagent was added at least 4 days prior to the iodonium carboxylate in the presence of [Cu(CH(3)CN)(4)]PF(6). The expected sulfonyl carboxylates were prepared and identified spectroscopically. NMR analysis of the products revealed the presence of multiple, conformationally restricted aromatic systems, presumably derived from the initial iodonium carboxylate partner.Q:
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I don’t have a strong working in physics neither I know which part of it to ask. I hope I can be of help.
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